王佳文,刘敏,邓春明,毛杰,韩伟,曾德长.等离子喷涂制备 ZrB2-SiC 复合涂层及其静态烧蚀性能[J].装备环境工程,2016,13(3):43-47. WANG Jia-wen,LIU Min,DENG Chun-ming,MAO Jie,HAN Wei,ZENG De-chang.Static Ablation Resistance of ZrB2-SiC Composite Coatings Prepared by Atmospheric Plasma Spraying[J].Equipment Environmental Engineering,2016,13(3):43-47.
等离子喷涂制备 ZrB2-SiC 复合涂层及其静态烧蚀性能
Static Ablation Resistance of ZrB2-SiC Composite Coatings Prepared by Atmospheric Plasma Spraying
投稿时间:2016-01-28  修订日期:2016-06-15
DOI:10.7643/ issn.1672-9242.2016.03.007
中文关键词:  C/C 复合材料  ZrB2-SiC 复合涂层  抗高温氧化  等离子喷涂
英文关键词:C/C composites  ZrB2-SiC composite coatings  oxidation resistance at high temperature  plasma spraying
基金项目:973 项目(2012CB625100),广东省科技项目(2013B050800031, 2014B050502008)
作者单位
王佳文 1.华南理工大学 材料科学与工程学院,广州 510640; 2.广东省新材料研究所,广州 510650;3.现代材料表面工程技术国家工程实验室,广州 510650;4.广东省现代材料表面工程重点实验室,广州 510650 
刘敏 1.广东省新材料研究所,广州 510650;2.现代材料表面工程技术国家工程实验室,广州 510650;3.广东省现代材料表面工程重点实验室,广州 510650 
邓春明 1.广东省新材料研究所,广州 510650;2.现代材料表面工程技术国家工程实验室,广州 510650;3.广东省现代材料表面工程重点实验室,广州 510650 
毛杰 1.广东省新材料研究所,广州 510650;2.现代材料表面工程技术国家工程实验室,广州 510650;3.广东省现代材料表面工程重点实验室,广州 510650 
韩伟 1.华南理工大学 材料科学与工程学院,广州 510640; 2.广东省新材料研究所,广州 510650;3.现代材料表面工程技术国家工程实验室,广州 510650;4.广东省现代材料表面工程重点实验室,广州 510650 
曾德长 华南理工大学 材料科学与工程学院,广州 510640 
AuthorInstitution
WANG Jia-wen 1.South China University of Technology, School of Material Science and Engineering, Guangzhou 510640, China;2.Guangdong Institute of New Materials, Guangzhou 510650, China;3.National Engineering Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China;4.Guangdong Provincial Key Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China 
LIU Min 1.Guangdong Institute of New Materials, Guangzhou 510650, China;2.National Engineering Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China;3.Guangdong Provincial Key Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China 
DENG Chun-ming 1.Guangdong Institute of New Materials, Guangzhou 510650, China;2.National Engineering Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China;3.Guangdong Provincial Key Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China 
MAO Jie 1.Guangdong Institute of New Materials, Guangzhou 510650, China;2.National Engineering Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China;3.Guangdong Provincial Key Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China 
HAN Wei 1.South China University of Technology, School of Material Science and Engineering, Guangzhou 510640, China;2.Guangdong Institute of New Materials, Guangzhou 510650, China;3.National Engineering Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China;4.Guangdong Provincial Key Lab for Modern Materials Surface Engineering Technology, Guangzhou 510650, China 
ZENG De-chang South China University of Technology, School of Material Science and Engineering, Guangzhou 510640, China 
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中文摘要:
      目的 提高 C/C 复合材料的抗静态烧蚀性能。 方法 利用大气等离子喷涂技术在 C/C 复合材料表面制备 ZrB2-SiC 复合涂层,对其进行 1500 ℃的静态烧蚀实验。利用 X 射线衍射仪(XRD)、扫描电子显微镜(SEM)及能谱分析仪(EDS)对涂层的物相成分、微观形貌等进行检测分析。 结果 采用大气等离子喷涂制备的 ZrB2-SiC 涂层是由熔融的粉末粒子紧密堆积而成,呈现典型的层状结构,涂层均匀完整地覆盖于 C/C基体表面,厚度约为200 μm。涂覆有 ZrB2-SiC复合涂层的 C/C复合材料试样在 1500 ℃分别氧化 2, 3, 4 h 后,试样依旧保持完整, C/C 基体未遭受损伤,试样的质量增加率依次为 3.39%,2.95%, 4.25%。 结论 采用大气等离子喷涂技术能够在 C/C 复合材料表面制备出厚度均匀、结构致密的 ZrB2-SiC 复合涂层, ZrB2-SiC 复合涂层使 C/C 复合材料的抗静态烧蚀性能显著提高。
英文摘要:
      Object To improve the static ablation-resistance of C/C composites. Methods The ZrB2-SiC composite coatings were deposited on C/C composites by atmospheric plasma spraying (APS). Oxidation experiments were carried out at 1500 ℃ on the ZrB2-SiC coated C/C composites. After that, microstructures of the coatings were analyzed by XRD, SEM and EDS. Results The homogeneous ZrB2-SiC coatings prepared on the surface of C/C composites by APS showed typical layer structure, and the coatings were composed of molted powder particles with close packing. The thickness was about 200 μm. After oxidation at 1500 ℃ for 2 h, 3 h and 4 h, the coated specimen still kept intact and did not suffer any injury, the weight increase of C/C specimen was 3.39%, 2.95% and 4.25%, respectively. Conclusion The homogeneous and integrated ZrB2-SiC composite coatings could be fabricated on the surface of C/C composites by atmospheric plasma spraying (APS), and ZrB2-SiC composite coatings could effectively improve the oxidation-resistance of C/C composites.
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