Anti-ablative Properties of ZrB2-TiC Composite Coatings Deposited by Low Pressure Plasma Spraying (LPPS)
Received:May 30, 2019  Revised:June 20, 2019
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DOI:10.7643/issn.1672-9242.2019.10.003
KeyWord:low pressure plasma spraying  ZrB2-TiC composite coating  oxygen- acetylene torch  ablation performance
              
AuthorInstitution
WEN Bo Aerospace Research Institute of Materials & Processing Technology, Beijing , China
NI Li-yong Aerospace Research Institute of Materials & Processing Technology, Beijing , China
MA Kang-zhi Aerospace Research Institute of Materials & Processing Technology, Beijing , China
YANG Zhen-xiao Aerospace Research Institute of Materials & Processing Technology, Beijing , China
QU Dong Aerospace Research Institute of Materials & Processing Technology, Beijing , China
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Abstract:
      Objective To explore anti-ablative properties of ZrB2-TiC composite coatings prepared by LPPS. Methods ZrB2-TiC spherical powder available for LPPS was prepared by spray granulation. ZrB2-TiC composite coatings were prepared on high strength graphite by LPPS. The ablation resistance of the coating was tested by oxygen acetylene torch. The surface temperature of the coating was measured with an infrared thermometer. The surface and section morphologies, elements and phases of coatings were analyzed with SEM, EDS and XRD, respectively. Results ZrB2-TiC composite coating showed the plasma spraying in a lamellar structure. The porosity of coating was about 10.8% and the bonding strength between the coating and high strength graphite reached 5.4MPa, approximately. There were ZrTiB4 and ZrTiC2 new phases in the coating after spraying. After being ablated by oxygen-acetylene torch for 5 min at 2000 ℃, the coating was in good condition, without any crack and peeling; and the ablation depth reached only 2-5 μm. Conclusion High performance ZrB2-TiC composite coating could be prepared on graphite by LPPS, and the coating could effectively prevent ablation from the oxyacetylene flame.
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